Integrated supercritical fluid extraction and online ICP-MS nano-gram determination of titanium( iv ) using calixarene hydroxamic acid

Analytical Methods 2026

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Authors: Devarshi Thaker, Bignesh Thakur, Nirav C. Pandya, Yadvendra Kumar Agrawal
DOI: 10.1039/d5ay01960e
Cited by: 0
References: 21

Abstract

, respectively. Method precision, evaluated by repeatability studies, resulted in relative standard deviation values below 5%, while accuracy assessed through recovery experiments ranged from 96% to 104%. The proposed method was successfully applied to the determination of titanium in certified NBS geological reference materials and real samples, including steel, brass, and ilmenite, with results in good agreement with certified values. The developed SFE-ICP-MS approach offers a rapid, sensitive, and environmentally benign alternative for the ultra-trace determination of titanium in complex matrices.

Fields of Study & Subjects

Analytical chemistry methods development Analytical Chemistry and Chromatography Radioactive element chemistry and processing

Publication details

Journal / source
Analytical Methods
Volume
18
Issue
11
Pages
2299–2305
Publication date
1 January 2026
Language
EN