Synthesis of mn doped NiCo-LDH integrated with rGO

Metal Organic Frameworks (MOFs) offers a controlled synthesis of LDHs when used as precursors. By employing metal-organic frameworks (MOFs) as precursors, 3D porous Mn/NiCo-rGO LDHs with flower- and flake-like structure were successfully synthesized via hydrothermal method, yielding materials with tunable pore structures and enhanced surface areas for wide ranging applications. Well-defined flakes and flower-like morphology were confirmed through FE-SEM and HR-TEM. IR spectroscopy verified the existence of typical LDH functional groups, along with metal-oxygen and metal-hydroxide bonds, demonstrating that the MOF precursor was effectively transformed into the desired layered double hydroxide (LDH) structure.