Facile Method to Prepare TiO₂ and CuO/TiO₂ Heterojunction and its Investigation for MB Degradation

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Abstract

High-purity TiO2 and CuO/TiO2 nanocomposite systems were prepared via a simple polyol solvothermal method.The synthetic precursors for nanomaterials were titanium isopropoxide (TTIP) and copper nitrate trihydrate.Several characteristic techniques, including X -ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), energy-dispersive Xray spectroscopy (EDX), Fourier transform infrared (FTIR) spectroscopy, Brunauer-Emmett-Teller (BET) testing, and photoluminescence (PL) spectroscopy, were employed to investigate the as-synthesised nanomaterials.The findings showed that the undoped TiO2 and CuO/TiO2 composite samples exhibited a rice-like structure after heat treatment for 3 hours at 450 °C in an oven.The optimized MB degradation reached approximately 99.87% at 160 min, compared to bare TiO2 nanoparticles, which achieved approximately 93.81% after 180 min of UV irradiation.

Fields of Study & Subjects

TiO2 Photocatalysis and Solar Cells Advanced Photocatalysis Techniques Advanced oxidation water treatment

Publication details

Journal / source
Malaysian Journal of Chemistry
Volume
28
Issue
1
Publication date
13 February 2026
Language
EN