STUDY OF THE STRUCTURE AND SURFACE MORPHOLOGY OF ACTIVATED CARBON FROM BLACK CUMIN SEED MEAL (Nigella sativa L.)

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Authors: Milena Nedkova-Shtipska, Liliya Manoilova, Metodi Kirilov Mladenov, Hristo Georgiev, Kamelia Ruskova, Galia Gentscheva
Cited by: 1

Abstract

The present study explores the potential of black cumin seed meal (Nigella sativa L.) (a by-product of industrial oil extraction) to produce activated carbon. The meal was carbonized at 500°C and chemically activated with 85 % H₃PO₄ at 500°C for 1 h. The obtained materials were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM-EDS), and elemental analysis (C, H and N). FT-IR spectra revealed the formation of a carbonized structure with surface oxygenated and phosphate functional groups. SEM micrographs provided a visual indication of a developed surface morphology with finely distributed pores; however, this observation does not substitute for a quantitative pore structure analysis such as N₂-sorption/BET. The obtained results confirm that black cumin seed meal can be used as a promising material for activated carbon production under phosphoric acid activation.

Fields of Study & Subjects

Adsorption and biosorption for pollutant removal Nigella sativa pharmacological applications Adsorption diffusion and thermodynamic properties of materials

Publication details

Journal / source
Journal of Chemical Technology and Metallurgy
Publisher
University of Chemical Technology and Metallurgy
Volume
61
Issue
2
Pages
283–292
Publication date
4 March 2026